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verized in the most powerful planetary ball mill and in the Emax 50 ml grinding jar of zircomium oxide 110 g matching grinding balls mm Ø 10 g sample 15 ml 1% sodium phos phate After 30 minutes the d90 value of the Emax sample was 87 nm The planetary ball mill achieved a grind size of only 476 nm after this time excl cooling breaks

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